Dynamic Shear Rheometer
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Dynamic Shear Rheometer
Dynamic Shear Rheometer (DSR) is a specialized laboratory instrument used to measure the rheological properties—specifically the viscoelastic behavior—of materials like asphalt binders, polymers, and other fluids or semi-solids. It applies controlled oscillatory shear stress or strain to a sample and analyzes its response to determine parameters such as the complex shear modulus (G*, which combines elastic and viscous components) and phase angle (δ, which indicates the balance between elasticity and viscosity). The DSR is particularly vital in asphalt testing under standards like AASHTO T 315 for Superpave performance-graded (PG) binder specifications, simulating real-world pavement stresses at various temperatures (typically 3–88°C) and frequencies (e.g., 10 rad/s to mimic traffic loading).
Standard Following
AASHTO T 315
Key Components
The DSR apparatus typically includes the following modular components, often integrated into a single unit for precision and automation
COMPONENT | DETAILS |
Parallel Plates | Upper and lower metal disks (25-mm diameter for unaged/RTFO-aged asphalt; 8-mm for PAV-aged). Gap: 1 mm (25-mm plates) or 2 mm (8-mm plates). Apply shear to the sample |
Environmental Chamber | Air- or liquid-filled enclosure (Peltier device or water bath) for precise temperature control (±0.1°C) from -20°C to 150°C. |
Loading Device | Electromagnetic or pneumatic actuator for applying oscillatory shear stress/strain. Supports stress- or strain-controlled modes. |
Control & Data Acquisition System | Software-driven interface for automation, calibration, and real-time analysis. Includes transducers for torque, displacement, and normal force. |
Sample Preparation Tools | Silicone molds, heated trimming tools, and cleaning solvents (toluene, acetone) for specimen handling |
Optional Accessories | Tool master for quick geometry swaps, Quick Connect for fast setup, and reference fluids for calibration |
Setup And Operation
- Calibration: Verify loading device and temperature system every 6 months using standard reference fluids and thermometers.
- Sample Preparation: Heat binder to pourable state (e.g., 163°C), pour between preheated plates, trim excess, and set gap (e.g., 1 mm).
- Testing: Stabilize at test temperature for 10 minutes in the chamber. Run 10 conditioning cycles, then 10 data cycles at specified frequency/strain. Software auto-computes G* and δ.
- Cleanup: Wipe plates with solvents to prevent contamination.